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    β-Nitrostyrenes as Electrophiles in Parham Cyclization Chemistry. Reaction with o-Lithiobenzonitrile

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    Date
    2009-06
    Author
    Clarke, Adam J.
    Hunt, David A.
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    Abstract
    Abstract
    β-Nitrostyrenes react with o-lithiobenzonitrile, generated from the requisite aryl bromide at −100 °C by bromine–lithium exchange with n-butyllithium in THF, to afford 2-nitro-3-phenyl-3H-inden-1-ylamines resulting from 1,4-addition to the β-nitrostyrene followed by intramolecular capture of the resultant nitronate anion by the ortho-cyano functional group.
    Citation:
    Clarke A.J.; Hunt, D.A. “β-Nitrostyrenes as Electrophiles in Parham Cyclization Chemistry. Reaction with o-Lithiobenzonitrile,” Tetrahedron Lett. 2009, 50, 2949-2951.
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    URI
    http://dx.doi.org/10.1016/j.tetlet.2009.03.217
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